Formulation Of Instant Functional Collagen Drink With Date Seeds Coffee (Phoenix dactylifera) And Spices (Ginger, Cinnamon, Cardamom, Clove) Using The D-Optimal Mixture Design Method

Mutia Hanifa

Abstract


The functional food trend has grown rapidly since the Covid-19 pandemic, including products made from natural ingredients like herbal collagen drinks. This research aims to develop an optimal collagen drink formulation by adding date seed coffee with ginger, cinnamon, cardamom, and cloves as antioxidants to optimize collagen function.Optimization was carried out using the Design Expert-13 device with the optimization response of antioxidant activity (mg TE/100g) and water content (%). The results showed that the optimal formulation consisted ofdate seed coffee 35.57%; hydrolyzed collagen 25%; and spice mixture (ginger, cinnamon, cardamom, cloves) of 39.432% with a desirability value of 0.741.The optimal product was then instantiated using the spray drying method and compared with commercial products without instantiation and collagen addition.The optimal product has an IC50 antioxidant activity of 743.86 ppm and total phenols of 187.23 mg GAE/100g), with a water content of 3.35%, hygroscopicity of 7.76%, bulk density of 0.488 g/mL, and a dissolution time of 23.32 seconds. The results of the hedonic test on the optimal sample as a whole from 100 panelists were “rather like†to “like†with an average value of 3.17 with the most preferred attributes being the consistency and aroma of spices.


Keywords


Functional drinks;Collagen;Date seed coffee;Spices;design expert;Mixture D-Optimal

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References


Anandharamakrishnan, C., Ishwarya, S.P., 2015. Spray Drying Techniques For Food Ingredient Encapsulation, 1st Ed. Wiley. Https://Doi.Org/10.1002/9781118863985

AOAC, 2005. Method 935.14 And 992.24, In: Official Method Of Analysis. Association Of Officiating Analytical Chemists, Official Method Of Analysis. Washington DC.

Apriliyanti, M.W., Prasetyo, A.F., Santoso, B., 2017. Optimasi Perlakuan Pendahuluan Dan Pengeringan Untuk Meningkatkan Betasianin Teh Kulit Buah Naga.

Badan Pengawas Obat Dan Makanan Republik Indonesia, (BPOM), 2011. Peraturan Kepala Badan Pengawas Obat Dan Makanan Nomor HK.03.1.23.11.11.09605 Tahun 2011 Tentang Perubahan Atas Peraturan Kepala Badan Pengawas Obat Dan Makanan Nomor HK.00.06.51.0475 Tahun 2005 Tentang Pedoman Pencantuman Informasi Nilai Gizi Pada Label Pangan. BPOM RI, Jakarta.

Bilek, S.E., Bayram, S.K., 2015. Fruit Juice Drink Production Containing Hydrolyzed Collagen. J. Funct. Foods 14, 562–569. Https://Doi.Org/10.1016/J.Jff.2015.02.024

Caballero, B., Finglas, P.M., Toldrá, F. (Eds.), 2015. Encyclopedia Of Food And Health, 3rd Ed. Ed. Elsevier Science, Burlington.

Campos, L.D., Santos Junior, V.D.A., Pimentel, J.D., Carregã, G.L.F., Cazarin, C.B.B., 2023. Collagen Supplementation In Skin And Orthopedic Diseases: A Review Of The Literature. Heliyon 9, E14961. Https://Doi.Org/10.1016/J.Heliyon.2023.E14961

Chen, Y., Huang, A.X., Faber, I., Makransky, G., Perez-Cueto, F.J.A., 2020. Assessing The Influence Of Visual-Taste Congruency On Perceived Sweetness And Product Liking In Immersive VR. Foods 9, 465. Https://Doi.Org/10.3390/Foods9040465

Chindapan, N., Puangngoen, C., 2024. Comparative Evaluation Of Volatile Aroma Compounds Content Of Freeze-Dried And Spray-Dried Instant Coffees. Burapha Sci. J. 29, 647–671.

Dewantoro, A.A., Kurniasih, R.A., Suharto, S., 2019. Aplikasi Gelatin Sisik Ikan Nila (Oreochromis Niloticus) Sebagai Pengental Sirup Nanas. J. Ilmu Dan Teknol. Perikan. 1, 37–46. Https://Doi.Org/10.14710/Jitpi.2019.5246

Faldt, P., Bergenstahl, B., Carlsson, G., 1993. The Surface Coverage Of Fat On Food Powders Analyzed By Esca (Electron Spectroscopy For Chemical Analysis). Food Structure 12, 225–234.

Fathoni, R., Hafidz, A.R., 2023. Sintesis Maltodextrin Dari Pati Jagung Komersial Dengan Variasi Konsentrasi Enzim Alpha Amylase, Suhu Serta Waktu Hidrolisa Untuk Menguji Dextrose Equivalen Value. Jurnal Chemurgy 7.

Fikry, M., Yusof, Y.A., Al-Awaadh, A.M., Rahman, R.A., Chin, N.L., Mousa, E., Chang, L.S., 2019. Effect Of The Roasting Conditions On The Physicochemical, Quality And Sensory Attributes Of Coffee-Like Powder And Brew From Defatted Palm Date Seeds. Foods 8, 61. Https://Doi.Org/10.3390/Foods8020061

García-Carrasco, M., Valdez-Baro, O., Cabanillas-Bojórquez, L.A., Bernal-Millán, M.J., Rivera-Salas, M.M., Gutiérrez-Grijalva, E.P., Heredia, J.B., 2023. Potential Agricultural Uses Of Micro/Nano Encapsulated Chitosan: A Review. Macromol 3, 614–635. Https://Doi.Org/10.3390/Macromol3030034

Gawałek, J., 2022. Spray Drying Of Chokeberry Juice—Antioxidant Phytochemicals Retention In The Obtained Powders Versus Energy Consumption Of The Process. Foods 11, 2898. Https://Doi.Org/10.3390/Foods11182898

Gengatharan, A., Rahim, M.H.A., 2023. The Application Of Clove Extracts As A Potential Functional Component In Active Food Packaging Materials And Model Food Systems: A Mini-Review. Appl. Food Res. 3, 100283. Https://Doi.Org/10.1016/J.Afres.2023.100283

Ghaffar, R.M., 2021. Pasundan Food Technology Journal (PFTJ), Volume 8, No.1, Tahun 2021 8.

Ghnimi, S., Umer, S., Karim, A., Kamal-Eldin, A., 2017. Date Fruit ( Phoenix Dactylifera L.): An Underutilized Food Seeking Industrial Valorization. NFS J. 6, 1–10. Https://Doi.Org/10.1016/J.Nfs.2016.12.001

Hariyadi, P., 2024. Tantangan 2024: Urgensi Transformasi Sistem Pangan. Dep. Ilmu Dan Teknol. Panganfakultas Teknol. Pertan. Dan SEAFAST Cent. IPB Univ. 19, 22–33.

Huda, S., 2020. Efek Evaporasi Dan Suhu Pengeringan Spraydrying Terhadap Karakteristik Fisik Dan Kimia Whey Bubuk. J. Teknol. Has. Pertan. 13, 84. Https://Doi.Org/10.20961/Jthp.V13i2.42716

Joshi, S., Mohapatra, A., Singh, L., Sahu, J.K., 2022. Spray Drying: Principles And Applications, In: Kumar, N., Panghal, A., Garg, M.K. (Eds.), Thermal Food Engineering Operations. Wiley, Pp. 141–177. Https://Doi.Org/10.1002/9781119776437.Ch5

Jumina, J., Siswanta, D., Zulkarnain, A.K., Triono, S., Priatmoko, P., Yuanita, E., Fatmasari, N., Nursalim, I., 2019. Development Of C-Arylcalix[4]Resorcinarenes And C-Arylcalix[4]Pyrogallolarenes As Antioxidant And UV-B Protector. Indones. J. Chem. 19, 273. Https://Doi.Org/10.22146/Ijc.26868

Kardas, M., Rakuła, M., Kołodziejczyk, A., Staśkiewicz-Bartecka, W., 2024. Consumer Preferences, Sensory Evaluation, And Color Analysis Of Beetroot And Tomato Juices: Implications For Product Development And Marketing In Health-Promoting Beverages. Foods 13, 4059. Https://Doi.Org/10.3390/Foods13244059

Kwapińska, M., Zbiciński, I., 2006. Prediction Of Final Product Properties After Cocurrent Spray Drying. Drying Technology: An International Journal 23, 1653–1665. Https://Doi.Org/10.1081/DRT-200065075

Lee, J.K.M., Taip, F.S., Abdullah, Z., 2018. Effectiveness Of Additives In Spray Drying Performance: A Review. Food Res. 2, 486–499. Https://Doi.Org/10.26656/Fr.2017.2(6).134

Lee, Y.I., Lee, S.G., Jung, I., Suk, J., Lee, M.-H., Kim, D.-U., Lee, J.H., 2022. Effect Of A Topical Collagen Tripeptide On Antiaging And Inhibition Of Glycation Of The Skin: A Pilot Study. Int. J. Mol. Sci. 23, 1101. Https://Doi.Org/10.3390/Ijms23031101

León-López, A., Morales-Peñaloza, A., Martínez-Juárez, V.M., Vargas-Torres, A., Zeugolis, D.I., Aguirre-Ãlvarez, G., 2019. Hydrolyzed Collagen—Sources And Applications. Molecules 24, 4031. Https://Doi.Org/10.3390/Molecules24224031

Maqsood, S., Adiamo, O., Ahmad, M., Mudgil, P., 2020. Bioactive Compounds From Date Fruit And Seed As Potential Nutraceutical And Functional Food Ingredients. Food Chem. 308, 125522. Https://Doi.Org/10.1016/J.Foodchem.2019.125522

Maramy, N.V., Widyaningsih, T.D., Martati, E., Zafira, Z., 2024. Formula Optimization Of Traditional Functional Beverage Minasarua From Bima West Nusa Tenggara Indonesia. Trends Sci. 21, 7693. Https://Doi.Org/10.48048/Tis.2024.7693

Meilgaard, M.C., 2016. Sensory Evaluation Techniques. CRC Press.

Mrabet, A., Jiménez-Araujo, A., Guillén-Bejarano, R., Rodríguez-Arcos, R., Sindic, M., 2020. Date Seeds: A Promising Source Of Oil With Functional Properties. Foods 9, 787. Https://Doi.Org/10.3390/Foods9060787

Mugendiran, V., Gnanavelbabu, A., Ramadoss, R., 2014. Parameter Optimization For Surface Roughness And Wall Thickness On AA5052 Aluminium Alloy By Incremental Forming Using Response Surface Methodology. Procedia Eng. 97, 1991–2000. Https://Doi.Org/10.1016/J.Proeng.2014.12.442

Nasution, A.N., Fitrisia, R., Tio, S., Girsang, E., Mutia, M.S., 2023. Formulation And Characterization Of Amomum Compactum Sol. Ex Maton Nano Emulsion And Its Antibacterial And Wound Healing Activity. J. Penelit. Pendidik. IPA 9, 10656–10662. Https://Doi.Org/10.29303/Jppipa.V9i12.5773

Plank, D.W., Szpylka, J., Sapirstein, H., Woollard, D., Zapf, C.M., Lee, V., Chen, C.-Y.O., Liu, R.H., Tsao, R., Düsterloh, A., Baugh, S., Collaborators:, 2012. Determination Of Antioxidant Activity In Foods And Beverages By Reaction With 2,2′-Diphenyl-1-Picrylhydrazyl (DPPH): Collaborative Study First Action 2012.04. J. AOAC Int. 95, 1562–1569. Https://Doi.Org/10.5740/Jaoacint.CS2012_04

Prasad, S., Tyagi, A.K., 2015. Ginger And Its Constituents: Role In Prevention And Treatment Of Gastrointestinal Cancer. Gastroenterol. Res. Pract. 2015, 1–11. Https://Doi.Org/10.1155/2015/142979

Pudziuvelyte, L., Marksa, M., Jakstas, V., Ivanauskas, L., Kopustinskiene, D.M., Bernatoniene, J., 2019. Microencapsulation Of Elsholtzia Ciliata Herb Ethanolic Extract By Spray-Drying: Impact Of Resistant-Maltodextrin Complemented With Sodium Caseinate, Skim Milk, And Beta-Cyclodextrin On The Quality Of Spray-Dried Powders. Molecules 24, 1461. Https://Doi.Org/10.3390/Molecules24081461

Ramadhani, L.I., Kusuma, S.M., Andriana, S.P., 2024. The Effect Of Maltodextrin Concentration And Drying Temperature On The Instant Coffee Production With Spray Drying Method. International Journal Of Applied Technology Research 05, 194–204. Https://Doi.Org/10.35313/Ijatr.V5i3.193

Ridwan Taher Lubis, Minda Sari Lubis, Gabena Indrayani Dalimunthe, Rafita Yuniarti, 2023. FORMULASI SEDIAAN MINUMAN SERBUK JELI LIDAH BUAYA (Aloe Vera (L.) Burm.F.). FARMASAINKES J. Farm. SAINS Dan Kesehat. 2, 178–188. Https://Doi.Org/10.32696/Fjfsk.V2i2.1889

Rogers, L., 2018. Sensory Panel Management, Woodhead Publishing Series In Food Science, Technology And Nutrition. Woodhead Publishing.

Romulo, A., Aurellia, C.A., 2024. Different Concentrations Of Maltodextrin And Albumin Influenced The Quality Characteristics And Hedonic Acceptance Of Sorghum Powder Drinks. IOP Conf. Ser. Earth Environ. Sci. 1338, 012029. Https://Doi.Org/10.1088/1755-1315/1338/1/012029

Sabariman, M., Sandrasari, D.A., Azni, I.N., Permata, T.D., 2021. Aplikasi Metode Mixture Design Pada Formulasi Minuman Fungsional Serbuk Temulawak, Jahe Merah Dan Gula Merah. J. Teknol. Pangan Dan Kesehat. J. Food Technol. Health 3, 41–48. Https://Doi.Org/10.36441/Jtepakes.V3i1.533

Stone, H., Bleibaum, R.N., Thomas, H.A., 2021. Affective Testing, In: Sensory Evaluation Practices. Elsevier, Pp. 297–336. Https://Doi.Org/10.1016/B978-0-12-815334-5.00004-5

Triandita, N., Maifianti, K.S., Rasyid, M.I., Yuliani, H., Angraeni, L., 2020. Pengembangan Produk Pangan Fungsional Dalam Meningkatkan Kesehatan Dan Kesejahteraan Masyarakat Di Desa Suak Pandan Aceh Barat. Logista - J. Ilm. Pengabdi. Kpd. Masy. 4, 457–464. Https://Doi.Org/10.25077/Logista.4.2.457-464.2020

Wang, X., Wang, T., Nepovimova, E., Long, M., Wu, W., Kuca, K., 2022. Progress On The Detoxification Of Aflatoxin B1 Using Natural Anti-Oxidants. Food Chem. Toxicol. 169, 113417. Https://Doi.Org/10.1016/J.Fct.2022.113417

Wijayanti, N., Widyaningsih, T.D., Wulan, S.N., Rifai, M., 2024. Influence Of Spray Drying Inlet Temperature On The Physical Properties And Antioxidant Activity Of Black Garlic Extract Powder. TRENDS IN SCIENCES 21. Https://Doi.Org/10.48048/Tis.2024.7247

Wu, M., Cronin, K., Crane, J.S., 2024. Biochemistry, Collagen Synthesis, In: Statpearls. Statpearls Publishing, Treasure Island (FL).

Yanti, F., Dharmayanti, N., Suryanti, S., 2022. Aktivitas Antioksidan Kolagen Dari Kulit Ikan Patin (Pangasius Sp.) Dengan Enzim Bromelin Kasar Kulit Nanas (Ananas Comosus L.): Antioxidant Activity Of Collagen From The Skin Of Pangas Catfish (Pangasius Sp) With Crude Bromelain Enzyme Of Pineapple Peel. J. Pengolah. Has. Perikan. Indones. 25, 88–96. Https://Doi.Org/10.17844/Jphpi.V25i1.36731




DOI: https://doi.org/10.14421/biomedich.2025.142.911-919

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Biology, Medicine, & Natural Product Chemistry
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